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By Aris Doelman, Annie R. Gregges, Edward M. Barrall II (auth.), Roger S. Porter, Julian F. Johnson (eds.)

Thermal research cuts a huge swathe via modern technology. inside of this area, advances in instrumentation allow the appliance of quantitative calorimetry to the total spectrum of recent fabrics. this is illustrated possibly no greater than via the set of contributions which make up this quantity four of Analytical Calorimetry. The examine supported during this fourth quantity of Analytical Calorimetry covers a wide selection of subject matters. the variety shows the sophistication which thermal research is achieving and extra­ ly the ever-widening purposes which are being built. The contributions to the amount characterize, partly, papers awarded sooner than the department of Analytical Chemistry on the Fourth Symposium on Analytical Chemistry held on the 172nd nationwide assembly of the yankee Chemical Society, August 29 - September three, 1976. numerous extra key contributions are integrated by means of favourite employees within the box. Julian F. Johnson Roger S. Porter v Quantitative Scanning Calorimetry with automatic info Acquisition and relief . . . . . . . 1 Aris Doelman, Annie R. Gregges, and Edward M. Barrall, II Thermodynamic houses of a sequence of P-N-Alkyl-P'-Cyanobiphenyls 19 E. M. Barrall II, R. J. Cox, A. Doelman, N. Clecak, J. A. Logan, and A. R. Gregges Thermodynamic homes of a sequence of 37 P-N-Alkoxy-P'-Cyanobiphenyls R. J. Cox, E. M. Barrall II, A. Doelman, N. J. Clecak, J. A. Logan, R. D. Diller, and A. R. Gregges a brand new Equation for Predicting Polyethylene Lifetimes from Thermal info fifty one Cary F.

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REFERENCES 1. Gray, G. , Harrison, K. J. and Nash, J. , Electron. Lett. 1, 130 (1973). 2. Gray, G. , Harrison, K. , Nash, J. , Hulme, D. , Korton, J. and Raynes, E. , Proceedings of the Symposium on Ordered Fluids and Liquid Crystals, R. S. Porter and J. F. , Interscience, New York (1974), p. 617. 3. Gray, G. , Harrison, K. J. and Nash, J. , Pramana, Suppl. 1, 381 (1975). 4. Hulme, D. , Raynes, E. P. and Harrison, K. , J. Chern. Soc. Chern. Commun. 1974, 98. 5. Kahn, F. , Appl. Phys. Lett. 6. Haas, W.

A vertical line was dropped between the two endotherms and a smooth baseline constructed from the onset of the smectic+uematic transition and the end of the nematic+isotropic liquid transition. The area so defined on the low temperature side was assigned to the smectic+uematic transition, and a corresponding operation was carried out on the high temperature side for the nematic+isotropic liquid. The total area under both peaks is also shown on Figure 9 as a hexagon. p-n-Decyl-p'-cyanobiphenyl: The purity of this material is lower than the preceding two members.

Kokta (5) ruled out completely the use of thermal analysis or oxygen uptake for lifetime predictions. The difficulties encountered using extrapolated data are mirrored in studies strictly for comparison testing. Despite early optimism (10,11) and recent claims (12), single point induction times obtained for variously stabilized polyethylene samples have not correlated with either oven aging or field experience. O'Rell and Patel (13) found no correlation between induction times measured at 200 0 with oven aging conducted at 120 0 • Several other investigators have reported on the same problem (14,5).

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